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Theory and practice of archaeological residue analysis

Auteur--

EditorBarnard H. & Eerkens J.W.

Jaar2007

PublicatietypeBoek

SerieBAR British Archaeological Reports International Series

Volume1650

Subtitel--

Pagina’s274

UitgeverArchaeopress

PlaatsOxford

ISBN9781407300849

Citation key--

Trefwoorden--

Plaatsgegevens

Exemplaar70823 ReknummerT-4-3-e

Inhoud
Introduction 1-7
Eerkens J.W & Barnard R.G.
  • Growth of Residue Studies , pp. 1-5
  • Scope of the Current Volume , pp. 5-7

Residues of Maize in North American Pottery: What Phytoliths can add to the story of Maize 9-18
Lusteck R.K. & Thompson R.G.
  • Materials and Methods , pp. 9-11
  • Results , pp. 12-15
  • Conclusions , p. 15

Micro-Residues on Stone Tools: The Bigger Picture from a South African Middle Stone Age Perspective 18-28
Lombard M. & Wadley L.
  • How Blind Tests improved our Method , pp. 19-21
  • Zooming Out , p. 21
  • Conclusion , p. 22

Methods of Interpreting Bronze Age Vessel Residues: Discussion, Correlation and the Verification of Data 29-41
Shishlina N.I., Borisov A.V., Bobrov A.A. & Pakhomov M.M.
  • Cultural Context , p. 29
  • Methodology , p. 30
  • Determination of Phosphate Residues , p. 31
  • Archaeobotanical Analyses , pp. 32-35
  • Results , p. 36
  • Interpretation of the Results , p. 36
  • Discussion and Recommendations , p. 38
  • Conclusions , p. 39

An Introduction to Archaeological Lipid Analysis by GC/MS 42-60
Barnard H., Dooley A.N. & Faull K.F.
  • Lipids and Fatty Acids , pp. 42-45
  • Extraction of an Archaeological Sample , p. 46
  • Additional Treatment of the Sample , p. 47
  • Gas Chromatography (GC) , pp. 48-49
  • Mass Spectometry (MS) , pp. 50-55
  • Interpretation of GC/MS-results , p. 56

Elucidating Pottery Function using a Multi-Step Analytical Methodology combining Infrared Spectroscopy, Chromatographic Procedures and Mass Spectometry 61-75
Regert M.
  • Organic Remains and Pottery Production , p. 62
  • Organic Remains and Pottery Function , p. 63
  • Organic Remains and Pottery Repair , p. 63
  • Interpreting Analytical Data , pp. 66-67
  • Description of Samples , pp. 68-70
  • Pottery with Tars of Resins , p. 71
  • Conclusions , p. 72

Fatty Acid Analysis of Archaeological Residues: Procedures and Possibilities 77-88
Malainy M.E.
  • Previous Research , p. 77
  • Development of the Identification Criteria , pp. 78-80
  • Testing the Validity of Identification Criteria , p. 81
  • Experimental Procedures , p. 81
  • Oven Storage of Cooking Residues , pp. 82-83
  • Soil Storage of Cooking Residues , pp. 84-85
  • Sample Selection and Handling Guidelines , pp. 86-87
  • Conclusions , p. 88

Organic Residue Analysis and the Decomposition of Fatty Acids in Ancient Potsherds 90-98
Eerkens J.W.
  • Organic Residue Analysis , p. 90
  • Decomposition: Food Sciences Perspective , p. 91
  • Decomposition: Archaeological Perspective , p. 92
  • Dealing with Decomposition , p. 92
  • Fatty Acid Ratios , p. 93
  • Conclusions , p. 94

A comparative Study of Extractable Lipids in the Sherds and Surface Residual Crusts of Ceramic Vessels from Neolithic and Roman Iron Age Settlements in the Netherlands 99-124
Oudemans T.F.M. & Boon J.J.
  • Introduction: Lipid Analysis in Ceramic Studies , p. 99
  • Introduction: Types of Residues , p. 99
  • Experimental: Sample Material and Treatment , p. 100
  • Experimental: Sample Material and Treatment , p. 100
  • Experimental: Instrumentation , p. 100
  • Results: Quantification , p. 101
  • Results: CHN Analysis , p. 104
  • Results: Qualitative Lipid Analusis , p. 104
  • Results: Quantitative Lipid Analysis , pp. 105-107
  • Discussion: Lipid Quantification , p. 108
  • Discussion: Chemotaxonimic Markers , pp. 108-109
  • Discussion: Lipid Preservation and Degradation , p. 110
  • Discussion: Possible Origin of Lipids , p. 111
  • Discussion: Lipids from Surface Residues , p. 111
  • Discussion: Lipids Absorbed in Ceramics , p. 112
  • Discussion: Chars from Other Sites , p. 112
  • Conclusions , p. 113

Patterns of Substinence Change During the Final Neolithic in the Primorye Region of the Russian Far East as Revealed by Fatty Acid Residue Analysis 125-134
Cassidy J.
  • The Bronze Age in the Primorye Region , p. 126
  • Zera Lake , pp. 127-128
  • Macrobotanical Analysis , pp. 129-130
  • Fatty Acid Ceramic Residue Analysis , pp. 131-133
  • Conclusions , p. 134

Using Residue to Confirm Trade Connections at Pella, Jordan 138-147
Hoekman-Sites H.A.
  • Trade at Pella , pp. 138-139
  • Theory behind Derivatization , p. 140
  • Sample Selection and Preparation , p. 141
  • Procedures and Criteria , p. 142
  • IR and GC/MS Resukts , p. 142
  • Interpretation of the Results , p. 143
  • Specific Plant Identification , pp. 144-145
  • Conclusions , p. 146

The Well-Tempered Pottery Analysis: Residue and Typological Analysis of Potsherds from the Lower Mississippi Valley
Reber E.A.
  • Archaeological Background , p. 148
  • Description of Sites , pp. 149-150
  • Methods , p. 151
  • Results , pp. 152-155
  • Discussion , pp. 156-157
  • Conclusions , p. 158

Analysis of Lipid Residues in Archaeological Artifacts: Marine Mammal Oil and Cooking Practices in The Arctic 161-178
Solazzo C. & Erhardt D.
  • Cooking Practices in the Arctic Coastal Areas , pp. 161-162
  • The Artifacts , p. 163
  • Archaeological Samples , p. 163
  • Modern Specimens , pp. 165-166
  • Analitycal Methods , p. 167
  • Fatty Acid Profiles in Modern Specimens , pp. 167-169
  • HTGC Results of the Archaeological Samples , p. 170
  • GC/MS Results of the Archaeological Samples , p. 170
  • The Samples from Miyowagh , pp. 171-172
  • Artifacts from Alaska ans Labrador , pp. 173-176
  • Discussion , p. 177

The Archaeology of Alkaloids 179-188
Rafferty S.M.

Reconstructing Mississippian Diet in the American Bottom with Stable Isotope Ratios of Pot Sherd Residues 189-199
Beehr D.E. & Ambrose S.H.
  • Cahokia and its Neighbors , pp. 190-191
  • Diet Reconstruction , p. 192
  • The Archaeological Sites , p. 192
  • Methods and Results on Untreated Samples , pp. 193-194
  • Methods and Results on Treated Samples , p. 195
  • Discussion and Conclusions , p. 196

Results of Seven Methods for Organic Residue Analysis Applied to One Vessel with the Residue of a Known Foodstuff 200-215
Barnard H., Ambrose S.H., Beehr D.E., Forster M.D., Lanehart R.E., Malainey M.E., Parr R.E., Rider M., Solazzo C. & Yohe R.M. II
  • Birth of the Round Robin , pp. 200-202
  • Camels and Camel Milk , p. 203
  • The Analysis of Camel Milk Residues , p. 204
  • Results of the Round Robin: Stable Isotopes , pp. 205-206
  • Results of the Round Robin: Proteins , p. 207
  • Results of the Round Robin: Lipids , pp. 208-210
  • Discussion , pp. 211-212

Introduction to the Analysis of Protein Residues in Archaeological Ceramics 216-231
Barnard H., Shoemaker L., Rider M., Craig O.E., Parr R.E., Sutton M.Q & Yohe R.M. II
  • The Preservation of Proteins , p. 216
  • Proteins as Archaeological Biomarkers , p. 217
  • Extraction of Archaeological Proteins , p. 218
  • Immunological Detection , pp. 218-219
  • Gel Separation and Proteomics , pp. 220-221
  • First Case Study: Cannibalism at Cowboy Wash , p. 222
  • Second Case Study: Proteins on Stone Tools , p. 223
  • Third Case Study: The Origins of Dairying , p. 124
  • Fourth Case Study: Proteins in Paint Media , p. 224
  • Fifth Case Study: the Round Robin , pp. 225-226
  • Discussion , p. 227

Appendix I: Common Isotopes of 99 Elements 232-235

Apendix II: A Short Overviuw of Protein Biochemistry 236-253
  • Transcription , pp. 238-239
  • Translation , p. 240
  • Post-translational Modifications , pp. 240-241
  • Mutation , p. 242
  • Antibodies , p. 243
  • Chirality , p. 244
  • Denaturation, Decomposition and Diagenesis , pp. 245-246
  • Collisionally Induced Dissociation , p. 247
  • Glossary , pp. 248-251
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